CHEM 2412 Laboratory
Section 20261
Organic Chemistry I Lab
Clayton College and State University
Instructor: Dr.
Michael J. Terapane
Office: A&S: 105-A
E-mail: michaelterapane@mail.clayton.edu
Web: http://a-s.clayton.edu/terapane
Phone: 770-960-4369
(office)
Class: M: 1:30-4:20pm
Office Hours:
Course Description: The main focus of this laboratory is to expose students to the most common techniques used for purification and analyzing organic compounds. In addition, students will gain experience in organic synthesis.
Credit Hours: 1.0 semester credit
hour
Course Requirements:
Prerequisites:
CHEM 1211/1211L, CHEM 1212/1212L, CHEM 2411/2411L
Corequisites: CHEM 2412
Text: Organic Experiments by Fieser and Williamson, 8th Ed., Heath
Supplies: Bound Laboratory Notebook (sewn-in pages) and Lab Safety Glasses
University Computer Requirement:Computer
Skill Prerequisites:
Able to use the WindowsTM operating system.
Able to use the Microsoft WordTM word processing program.
Able to send and receive e-mail using OutlookTM or Outlook ExpressTM.
Able to use a Web browser.
Course
Objectives:
To learn laboratory techniques used in
organic chemistry
To learn, perform and analyze the
spectroscopic methods commonly used in the identification of
organic compounds
Student
Learning Outcomes
General education outcomes:
Communication: knowledge base. CHEM
2412L will provide knowledge base information
necessary for communication of information concerning principles of organic
chemistry.
Critical
Thinking: Question/Issue, Method, Evidence, Conclusion.
CHEM 2412L will provide problem solving skills needed in an organic
chemistry laboratory. Students will
be required to assess information obtain during laboratory experimentation and
form a conclusion based on that information.
In this process, students will be required to determine which given
information is pertinent and if their conclusion is reasonable.
Applied Biology Outcomes:
Outcome 2: Students will be able to
effectively communicate scientific ideas using oral, written and digital arts.
CHEM 2411L will provide knowledge base information necessary for
communication of information concerning techniques used in the organic chemistry
laboratory.
Outcome 7: Students will obtain a
sufficient background in chemistry to pursue further professional education in
the biomedical field.
Course
Policies:
Students will obide by all policies set forth in the Clayton College and
State University Student Handbook
No extra credit assignments will be given, however, bonus questions are often included on examinations.
Attendance in required! Students missing a laboratory period will be assigned a grade of 0 for that lab experiment. Make-up lab experiments cannot be accommodated. Students who have a valid excused absence will have their other lab reports worth more in order to make up for the missed experiment.
In-class use notebook computers: Student notebook computers will not be used in the classroom in this course. However, students are responsible for checking their e-mail for schedule changes, updates, etc. Students from other universities are responsible for submitting their e-mail addresses to the instructor on the first day of class and expected to check them throughout the course. In addition, a computer is required to access the syllabus as well as other resources for the course.
Individuals with disabilities who need to request accommodations or obtain this document in an alternative format, contact Gina Phillips, Disability Services Coordinator, Student Center 214, 770-961-3719, ginaphillips@mail.clayton.edu.
Grading:
Exams: There will be two one-hour exams and 5 lab reports worth 100
points each.
Lab
Exam (1 x 100
points)
100 points
Lab Reports (4 x 100
points)
300 points
Total
Points
400 points
Final Grade = Points earned/500 x 100%
90-100%
= A
80-89% = B
70-79% = C
60-69% = D
< 60% = F
Tentative Schedule
|
Date |
Lab Period |
Experiment |
Text Reference |
|
6/26 |
Lab 1 |
Synthesis of Adipic Acid from cyclohexene |
Pgs. 254-256, 260-261 |
|
7/1 |
|
Lecture on Spectroscopy |
|
|
7/3 |
Lab 1 (Cont'd) |
Purification and Analysis of Adipic Acid |
Pgs. 371-5
|
|
7/8 |
Lab 2 |
Synthesis of Triphenylmethanol |
|
|
7/10 |
Lab 2 (Cont'd) |
Purification of Triphenylmethanol and IR analysis |
Pgs. 463-469 |
|
7/15 |
Lab 3 |
Friedel-Crafts Alkylation of Benzene and Dimethoxybenzene; Host-Guest Chemistry |
|
|
7/17 |
Lab Report 2 due |
Friedel-Crafts (Cont'd) |
Pgs. 299-302 |
|
7/22 |
Lab Report 3 due |
Lab Exam Check-Out |