CHEM 2411L - Organic Chemistry I

CHEM 2411L - Organic Chemistry I Laboratory
Course Syllabus - Summer 2009

Individuals with disabilities who need to request accommodations should contact
the Disability Services Coordinator, Student Center 214, 678-466-5445, disabilityservices@mail.clayton.edu.

Course Description:

Number and Title:

CHEM 2411L (CRN 53645)
Organic Chemistry I Laboratory

Credit Hours:

1.0 semester credit hours

Catalog Description:

A study of the common laboratory techniques used in synthesizing, purifying and analyzing organic compounds.

Course Prerequisite:

CHEM 1212, CHEM 1212L

Course Co-requisite:

Co-requisite: CHEM 2411

Note: Due to the co-requisite nature of CHEM 2411 and CHEM 2411L, students dropping one of the two courses must also drop the other.

Notebook Computer Requirement:

Each CSU student is required to have ready access throughout the semester to a notebook computer that meets faculty-approved hardware and software requirements for the student's academic program. Students will sign a statement attesting to such access. For further information on CSU's Official Notebook Computer Policy, please go to http://itpchoice.clayton.edu/policy.htm.

Computer Skill Prerequisites:

Able to use the computer’s operation system (Windows®)

Able to access and send e-mail (Outlook® or Outlook Express®)

Able to use a Web browser (Internet Explorer®) and search engine

Able to download files from a web site to your computer

Able to use a word processor system (Word®)

Able to use a spread sheet system (Excel®)

In-class Use of Student Notebook Computers:

Student notebook computers will not be used in the classroom in this course. Computers will be required to access course materials and to communicate with your instructor.

Course Objectives:

To learn laboratory techniques used in organic chemistry.
To learn perform and analyze the spectroscopic methods commonly used in an organic chemistry laboratory.

Student Learning Outcomes:

General education outcomes:

Communication: knowledge base. CHEM 2411L will provide knowledge base information necessary for communication of information concerning principles of organic chemistry.
Critical Thinking: Question/Issue, Method, Evidence, Conclusion. CHEM 2411L will provide problem solving skills needed in an organic chemistry laboratory. Students will be required to assess information obtain during laboratory experimentation and form a conclusion based on that information. In this process, students will be required to determine which given information is pertinent and if their conclusion is reasonable.

Biology Outcomes:

Outcome 3: Knowledge of physical science, mathematics, and statistics required to support an understanding of biology.
Outcome 4: Ability to communicate orally and in writing in a clear, concise manner.
Outcome 5: Ability to collect, evaluate and interpret scientific data, and employ critical thinking to solve problems in biological science and supporting fields.

Instructor Information:

Dr. Susan F. Hornbuckle
Phone: (678) 466-4780
E-mail: SusanHornbuckle@clayton.edu
Internet: http://a-s.clayton.edu/shornbuckle/default.html
Office: Faculty Hall: ADM-11

Office hours:

3:20 PM – 5:00 PM
(by appointment only)* MW ADM-11 or BHS:C-54

12:30 PM - 3:20 PM
(by appointment only)* W BHS:C-54

10:00 AM - 4:00 PM
(by appointment only)* T ADM-11

other times by appointment*

*You may phone, email or talk to me in person to make an appointment.

Class Meetings:

Day	Time	Room
M	12:30 PM - 3:20 PM	B&HS: C-54
M	3:20 PM - 6:10 PM	B&HS: C-54

Textbook Information:

Text:

Making the Connections: A How-To Guide for Organic Chemistry Lab Techniques by Anne B. Padias, 1st Ed.,
Thomson Laboratory Notebook with carbonless copies (Available in the bookstore)
Ink Pen

Supplies:

You are required to supply your own safety glasses for the laboratory. These are available in the campus book store but may be purchased elsewhere. Safety glasses MUST be worn in the laboratory at all times. If necessary, the instructor will deduct points from lab reports for not wearing safety glasses while in the laboratory. You will not be allowed to continue to work in the laboratory without safety glasses or your notebook.

Evaluation:

Your evaluation in CHEM2411L will be based upon the following components:

Component	points
Pre-Laboratory Questions (10 points each)	100
Laboratory Reports (50 points each)	500
Laboratory Notebook (5 points each)	40
Lab Exam (100 points)	100
Total	740

Grading:

The grade you receive in Chemistry 2411L will be based upon the following distribution:

letter grade	percentage range
A	90% or greater
B	80% - 89%
C	70% - 79%
D	60% - 69%
F	< 60%

Mid-term Progress Report

The mid-term grade in this course which will be issued on June 24th reflects approximately 30% of the entire course grade. Based on this grade, students may choose to withdraw from the course and receive a grade of "W." Students pursuing this option must fill out an official withdrawal form, available in the Office of the Registrar, by mid-term, which occurs on June 26th.

Tentative Course Schedule*:

Date	Turn in at start of lab	Turn in at end of lab	Lecture Topic
June 1	Safety Rules Liability Waiver		Syllabus Introduction to Lab Equipment and Safety Lab Check in
June 1	Exp. #1 Prelab		Exp. #1 - Literature of Organic Chemistry	p. 45-46
June 8 12:30pm	Exp. #1 Report Exp. #2 Prelab	Exp. #2 Lab notes	Exp. #2 - Melting Points	p. 47-51 handout
June 8 3:20pm	Exp. #3 Prelab	Exp. #3 Lab notes	Exp. #3 - Recrystallization	p. 107-109 handout
June 15 12:30pm	Exp. #2 Report Exp. #3 Report Exp. #4 Prelab		IR Spectroscopy Lecture Exp. #4 - IR Spectroscopy Lecture and Lab	p. 64-74 handout
June 15 3:20pm	Exp. #5 Prelab	Exp. #5 Lab notes	Exp. #5 - Extraction	p. 116-124 handout
June 22 12:30pm	Exp. #4 Report Exp. #5 Report Exp. #6 Prelab	Exp. #6 Lab notes	Chromatography Lecture Exp. #6 - Thin Layer Chromatography	p.150-152 p.153-159 handout
June 22 3:20pm	Exp. #7 Prelab	Exp. #7 Lab notes	Exp. #7 - Column Chromatography	p. 160-165 handout
June 29 12:30pm 3:20pm	Exp. #6 Report Exp. #7 Report Exp. #8 Prelab	Exp. #8 Lab notes	Exp. #8 - Steam Distillation of Essential Oils (Typically completed in two lab periods.)	p. 129-133 p. 141-143 handout
July 6 12:30pm	Exp. #8 Report Exp. #9 Prelab	Exp. #9 Lab notes	Exp. #9 - Nucleophilic Substitution of Alkyl halides	handout
July 6 3:20pm	Exp. #9 Report Exp. #10 Prelab	Exp. #10 Lab notes	Exp. #10 - Dehydration of Alcohols	handout
July 13 12:30pm	Exp. #10 Report		Lab Exam Lab Clean Up

*The instructor reserves the right to alter the course schedule at any time during the semester.

Important Dates

Last day to withdraw with academic penalty June 26th

Course Policies:

Pre-lab and Laboratory Reports:

There will be ten laboratory reports worth 50 points each and ten pre-lab assignments worth 10 points each. Pre-lab reports and laboratory reports are to be typed using the forms supplied to you at the course website. These reports are to be typed and structures are to be drawn using a computer chemical drawing program. Pre-lab reports and laboratory reports are due at the start of class (unless otherwise stated) on the assigned due dates. Reports turned in after the start of class will be treated as a day late (i.e. grade – 10%). Late reports will have 10% deducted for each school day it is past due. Reports over nine days late will not be accepted.

Attendance:

Attendance is required. Students missing a laboratory period will be assigned a grade of zero for assignment done that day. Make up laboratory experiences will be offered at the instructors convince and are only available to those students having valid excuses. Students should contact the instructor via telephone or e-mail within 24 hours of the missed lab to schedule a make up lab. After that time, no make up labs will be scheduled..

Laboratory Accidents:

Participation in laboratory activities involves an inherent risk of injury. In the event of injury, the student should immediately inform the instructor or laboratory technician who will file an accident report. The injured party will be given first aid through the Campus Public Safety Officer and be referred to the appropriate medical facility for follow-up.

Academic Irregularity:

Cheating in any form will not be tolerated. Consequences may include a zero grade on the assessment instrument, or possible action by the College Judicial Board of Review.

Disruption of the Learning Environment:

Behavior which disrupts the teaching–learning process during class activities will not tolerated. While a variety of behaviors can be disruptive in a classroom setting, more serious examples include belligerent, abusive, profane, and/or threatening behavior. A student who fails to respond to reasonable faculty direction regarding classroom behavior and/or behavior while participating in classroom activities may be dismissed from class. A student who is dismissed is entitled to due process and will be afforded such rights as soon as possible following dismissal. If found in violation, a student may be administratively withdrawn and may receive a grade of WF. A more detailed description of examples of disruptive behavior and appeal procedures is provided at:
http://a-s.clayton.edu/DisruptiveClassroomBehavior.htm

Other Class Policies:

"Students must abide by policies in the Clayton State University Student Handbook, and the Basic Undergraduate Student Responsibilities."

Arrive to lab on time and stay until the exercise is complete.

No children or visitors are allowed in the Laboratory.

Turn off phones, radios and other electronic devices.

No eating, smoking or drinking in the laboratory. No food is allowed in the laboratory.

Be aware of all policies and procedures.

No extra credit work will be assigned.

Grades will not be communicated via email or telephone.

Last update: April 20, 2009

Office hours:
	3:20 PM – 5:00 PM (by appointment only)*	MW	ADM-11 or BHS:C-54
	12:30 PM - 3:20 PM (by appointment only)*	W	BHS:C-54
	10:00 AM - 4:00 PM (by appointment only)*	T	ADM-11
	other times by appointment*

Important Dates
Last day to withdraw with academic penalty	June 26th