CHEM 2411L - Organic Chemistry I Lab
Course Syllabus - Fall 2009

Course Schedule



Individuals with disabilities who need to request accommodations should contact the 
Disability Services Coordinator, Student Center 255, 678-466-5445, disabilityservices@clayton.edu 



Course Description:

        Number and Title:

Chemistry 2411L (CRN 87196 or 87197)
Organic Chemistry Laboratory I

        Credit Hours:

          1.0 semester credit hours

        Catalog Description:

            A study of the common laboratory techniques used in synthesizing, purifying and analyzing organic compounds.

        Course Prerequisite:

          CHEM 1212 and CHEM 1212L

        Course Co-requisite:

          Co-requisite: CHEM 2411 (CRN 87195)

   
Note: Due to the co-requisite nature of CHEM 2411 and CHEM 2411L, students dropping one of the two courses must also drop the other.

        Computer Requirement:

Each CSU student is required to have ready access throughout the semester to a notebook computer that meets faculty-approved hardware and software requirements for the student's academic program. Students will sign a statement attesting to such access.  For further information on CSU's Official Notebook Computer Policy, please go to http://itpchoice.clayton.edu/policy.htm.

        Computer Skill Prerequisites:

  • Able to use the computer’s operation system (Windows®)
  • Able to send and receive e-mail (Outlook® or Outlook Express®)
  • Able to attach and retrieve attached files via email
  • Able to use a Web browser (Internet Explorer®) and search engine
  • Able to download files from a web site to your computer
  • Able to use a word processor system (Word®)
  • Able to use Microsoft PowerPoint®
  • Able to use a spread sheet system (Excel®)

In-class Use of Student Notebook Computers:

Student notebook computers will be used occasionally in the classroom in this course. Computers will also be required to access course materials and to communicate with your instructor.


Course Learning Outcomes:


Program Learning Outcomes:

        General education outcomes:

Biology Outcomes:

CHEM 2411L is a required course in the B.S. degree in biology. CHEM 2411L supports outcomes 3, 4, and 5 of the biology major.


Instructor Information:

Instructor:

Dr. Caroline Clower
Office phone: (678) 466-4777
Fax: (678) 466-4797
Office: Faculty Hall, Room A32
Email: CarolineClower@clayton.edu
Internet: http://a-s.clayton.edu/cclower/

Office hours: 
          
          Monday and Wednesday, 10:00 am - 12:00 pm
 
         or by appointment


Class Meetings:

CRN Day Times Room
87196 R 12:35 - 3:25 pm BHS C-54
87197 F 10:00 am - 12:50 pm BHS C-54

 


Textbook Information:

Text:

Making the Connections: A How-To Guide for Organic Chemistry Lab Techniques by Padias, Hayden-McNeil, 2007.

Supplies:

Carbonless Student Laboratory Notebook
Laboratory Safety Glasses


Evaluation:

Your evaluation in CHEM 2411L will be based upon the following components:  

component points
Laboratory Reports (9 @ 50 points)*

450

Lab Practical 50
Exam 100
TOTAL

600

            * Ten (10) laboratory reports will be submitted. The lowest laboratory report grade will be dropped.


 

Grading:

The grade you receive in Chemistry 2411L will be based upon the following distribution:

letter grade percentage range point range
A 90% or greater 540-600
B 80% - 89% 480-539
C 70% - 79% 420-479
D 60% - 69% 360-419
F less than 60% < 360

 


Mid-term Progress Report

Due to the relatively small number of laboratory reports that will have been returned by mid-term, mid-term grades may not be reported for this course.  If a mid-term grade is submitted, it will reflect approximately 30% of the entire course grade.  Based upon this grade, students may choose to withdraw from the course and receive a grade of "W."  Students pursuing this option must fill out an official withdrawal form, available in the Office of the Registrar, by mid-term, October 9, 2009.  Please note that if you withdraw from the laboratory, you must also withdraw from the lecture course.


Tentative Course Schedule:

        The instructor reserves the right to alter the course schedule as necessary and will communicate any changes clearly to the class.

Lab

Date Experiment to be performed Required Reading* Assignment Due**
  8/20-21 NO LAB      
  8/27-28

Introduction to the course, lab equipment and safety

pp. 1-44  
1 9/3-4 Melting Points pp. 47-50 Pre-lab 1
2 9/10-11 Recrystallization pp. 107-115 Pre-lab 2
Report 1
3 9/17-18 Extraction pp. 116-128 Pre-lab 3
Report 2
4 9/24-25 Literature of Organic Chemistry
(Meet in classroom)
  Pre-lab 4
Report 3
5 10/1-2 IR Spectroscopy (Meet in classroom for lecture, then proceed to lab for IR experiment) Padias, pp. 63-74
Wade, Chapter 12
Pre-lab 5
Report 4
 6 10/8-9 Chromatography (Meet in classroom for lecture, then proceed to lab for Thin Layer Chromatography experiment) Padias, pp. 150-159
Wade, Chapter 12
Pre-lab 6
Report 5
7 10/15-16 Column Chromatography pp. 160-165 Pre-lab 7
Report 6
 8 10/22-23 Steam Distillation of Essential Oils pp. 129-145 Pre-lab 8
Report 7
  10/29-30 Mass Spectrometry (Meet in classroom for lecture, then proceed to lab for continuation of Steam Distillation of Essential Oils experiment) pp. 98-106, 167-176  
9 11/5-6 Nucleophilic Substitution of Alkyl Halides   Pre-lab 9
Report 8
10 11/12-13 Dehydration of Alcohols   Pre-lab 10
Report 9
  11/19-20 Lab Practical Procedure on
course website
Report 10
  11/26-27 No Lab    
  12/3-4 Exam
Lab clean-up
(Attendance is mandatory)
   Lab Practical  

  * All required reading is from the Padias text unless otherwise indicated. Procedures, pre-lab questions, and report sheets for all experiments can be found on Dr. Clower's CHEM 2411L website.
** Assignments are due at the beginning of the lab period unless otherwise noted. The penalty for late reports is 10 percent per school day. Late pre-lab assignments will not be accepted.


Course Policies:

Pre-laboratory Assignments:

Pre-lab assignments are worth 5 points each and are counted as part of the report grade. These assignments are to be typed using the forms supplied to you at the course website. Structures must be drawn neatly be hand or using a software program (such as ChemDraw). Pre-lab assignments are due at the start of class on the day the experiment is to be performed. Late pre-lab assignments will not be accepted.

Laboratory Reports:

Laboratory reports are worth 50 points each.  Laboratory reports are to be typed using the form supplied to you at the course website.  Structures must be drawn neatly be hand or using a software program (such as ChemDraw).  Laboratory reports are due at the start of class (unless otherwise stated) on the assigned due dates. Reports turned in after the start of class will be treated as a day late.  Late reports will have 10 percent deducted for each school day it is past due.  Reports over nine days late will not be accepted. Your lowest laboratory report grade will be dropped.

Laboratory Practical:

The lab practical is an experiment designed to test your laboratory skills and technique. The practical will be performed individually during a regularly scheduled laboratory period at the end of the semester, and will require you to use separation, purification, spectroscopy and characterization methods learned in previous experiments.

Exam:

The laboratory exam is worth 100 points and will test you on experimental techniques, spectroscopy, and theory discussed in the laboratory.

Laboratory Notebook:

The laboratory notebook is your record of procedure notes, observations, and data. The duplicate pages will be collected at the end of each lab period and periodically graded for clarity and completeness. If you do not have your notebook with you in lab, or do not use the notebook to record your data (i.e. if you record data on another paper and copy it into your notebook), points may be deducted from that experiment's laboratory report.

Laboratory Safety and Accidents:

Laboratory safety rules will be discussed during the first laboratory meeting, and will be followed by all students in the course. Failure to follow these rules will result in deduction of points from your grade. Participation in laboratory activities involves an inherent risk of injury. In the event of injury, the student should immediately inform the instructor or laboratory technician who will file an accident report. The injured party will be given first aid through the Campus Public Safety Officer and be referred to the appropriate medical facility for follow-up.

University Attendance Policy

Students are expected to attend and participate in every class meeting. Instructors establish specific policies relating to absences in their courses and communicate these policies to the students through the course syllabi. Individual instructors, based upon the nature of the course, determine what effect excused and unexcused absences have in determining grades and upon students’ ability to remain enrolled in their courses. The university reserves the right to determine that excessive absences, whether justified or not, are sufficient cause for institutional withdrawals or failing grades.

Course Attendance Policy:

Attendance is required. Students missing a laboratory period will be assigned a grade of zero for assignment done that day. Make-up laboratory experiences will not be offered.

Academic Dishonesty:

Any type of activity that is considered dishonest by reasonable standards may constitute academic misconduct. The most common forms of academic misconduct are cheating and plagiarism. All instances of academic dishonesty will result in a grade of zero for the work involved. All instances of academic dishonesty will be reported to the Office of Student Life/Judicial Affairs. Judicial procedures are described at http://adminservices.clayton.edu/judicial/.

        Disruption of the Learning Environment

Behavior which disrupts the teaching–learning process during class activities will not tolerated. While a variety of behaviors can be disruptive in a classroom setting, more serious examples include belligerent, abusive, profane, and/or threatening behavior. A student who fails to respond to reasonable faculty direction regarding classroom behavior and/or behavior while participating in classroom activities may be dismissed from class. A student who is dismissed is entitled to due process and will be afforded such rights as soon as possible following dismissal. If found in violation, a student may be administratively withdrawn and may receive a grade of WF. A more detailed description of examples of disruptive behavior and appeal procedures is provided at: http://a-s.clayton.edu/cclower/Disruptive Classroom Behavior.doc.

Other Class Policies:

Students must abide by policies in the Clayton State University Student Handbook, and the Basic Undergraduate Student Responsibilities.

  • Arrive to lab on time and stay until the exercise is complete.
  • No children or visitors are allowed in the laboratory.
  • Turn off beepers, phones, radios and other electronic devices.
  • No eating, smoking or drinking in the laboratory. No food is allowed in the laboratory.
  • Be aware of all policies and procedures.
  • No extra credit work will be assigned.
  • Grades will not be communicated via email or telephone.


Last update: August 26, 2009